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Manufacturer
PAL GC Autosampler
 
Upgrade to ITXE-2 Mode
PAL COMBI-xt equipped with ITEX-2 Option
Get P&T sensitivity without cost of a P&T System
Rapid & efficient sample enrichment of volatile & semi-volatile compounds in solid, liquid and gaseous samples
In-tube extraction and direct thermal desorption using proven industry standard adsorbents
Syringe only concept for transparent sample handling, no sample loops, no transfer lines, no switching valves
Sample extraction procedure
 
ITEX-2 upgrade kit

CTC Analytic's objective is to supply instruments to customers which make the operation of sample processing simple and transparent. In-line with today’s lab requirements for productivity, CTC expanded the application range of its GC injector system PAL COMBI-xt introducing the ITEX-2 Option. The ITEX-2 Option consists of an add-on module which can be used with any existing or new PAL COMBI-xt Systems. It performs enrichment of volatile or semi-volatile compounds during headspace analysis. A microtrap filled with adsorbent material, such as Tenax or activated charcoal is placed between the heated PAL COMBI-xt Headspace syringe and the syringe needle. Using the HS syringe as a pump, a part of the gaseous phase of the pre-conditioned sample vial is pumped repeatedly through the microtrap. This system setup allows rapid, simple and efficient extraction of volatile and semi-volatile sample compounds. To gain sensitivity simply the number of pumping strokes can be increased or several different vials containing the same sample can be extracted. During thermal desorption into the GC injector the microtrap is rapidly flash heated and the analytes reach the GC column as a narrow band. No cryofocussing is needed to obtain sharp peaks. To prepare the next extraction, the hot trap is re-conditioned outside the injector with clean purge gas.

Detail
Consisting of 1pc  1.3ml ITEX syringe with M7 x 0.5 fitting
1pc  Replacement plunger 1.3ml
2pcs ITEX-2 trap TENAX TA 80/100 mesh incl. O-Ring
1pc  Trap Heater incl. electrical connections
1pc  Syringe heater incl. plunger holder
1pc  Syringe heater side bracket
1pc  CD ROM with ITEX software
       (requires Cycle Composer)
 
Specification
Pumping syringe size: 1.3ml HD Syringe with removable trap
ITEX-2 Trap: Stainless steel material, deactivated by Siltek ®
Standard trap material: 44mg Tenax TA 80/100 mesh
Needle: Injection needle gauge 23, Point style 5 (side hole)
Extraction speed: selectable from 10µl/sec up to 1000µl/sec
Extraction strokes: selectable from 1 – 999
Extraction volume: selectable from 130 µl - 1300µl/stroke
Desorption temperature: +5°C above ambient – 350°C selectable in 1°C increments
Heating-up rate: up to 12°C/sec
Desorption speed: 1µl/sec - 500µl/sec
Pumping syring and trap cleaning: Inert gas purging, 30sec – 3600min
Heated pumping syringe: +5°C above ambient – 150°C selectable in 1°C increments
Incubator oven: 6 heated vial positions for 2ml/10ml/20ml vials
  +5°C above ambient – 200°C selectable in 1°C increments
 
More information from CTC : http://www.palsystem.com/index.php?id=256
 
For more information contact : info@scispec.co.th
 
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